田国贺,王坤,韩晓红.参茸天麻酒的质量标准研究和探讨[J].中国药品标准,2020,21(1):26-31 |
参茸天麻酒的质量标准研究和探讨 |
Research and discussion on the quality standard ofShenrongtianma Medicinal Liquor |
投稿时间:2019-08-21 修订日期:2020-02-03 |
DOI: |
中文关键词: 参茸天麻酒 天麻素 质量标准 薄层色谱法 高效液相色谱法 |
英文关键词: Shenrongtianma Medicinal Liquor Gastrodin Quality Standard TLC HPLC |
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中文摘要: |
目的:完善参茸天麻酒的质量控制标准。方法:采用薄层色谱法对方中主要药味天麻、枸杞子、何首乌、人参和五味子展开鉴别考察,采用高效液相色谱法测定君药天麻中天麻素的含量。结果:薄层鉴别斑点清晰、分离度好、专属性强且重复性良好。天麻素含量测定方法操作简单、准确,天麻素的线性范围9.76μg.ml-1~97.6μg.ml-1(r=0.9999);精密度、稳定性、重复性试验的RSD<1.0%;加样回收率为99.7%(RSD=1.5%,n=6)。结论:定性、定量方法准确、简单,能有效控制参茸天麻药酒的质量。 |
英文摘要: |
ABSTRACT Objective: To improve the quality standard of Shenrongtianma Medicinal Liquor.Methods: TLC was applied for qualitative identification of Gastrodiae Rhizoma,Lycii fructus,Polygoni multiflori Radix,Ginseng Radix et Rhizoma and Schisandrae Chinensis Fructus.HPLC was used to determine the content of gastrodin. Results: The TLC chromatograms showed the characteristic spots were clear and good resolutions. The TLC methods we established are specific and with a good reproducibility.The HPLC method we established is simply, accurate and has a good linearity in the range of 9.76μg?ml-1~97.6μg?ml-1(r=0.9999), RSDs of precision, stability and reproducibility tests were all 1ower than 1.0%, The recovery was 99.7%(RSD=1.5%,n=6). Conclusion: The qualitative and quantitative methods we established are easy and accurate. It can be used for the quality control of Shenrongtianma Medicinal Liquor. |
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