王庆芬,倪晓霞,刘晓玲,郑绍忠.《中国药典》2015年版中纯化水硝酸盐检查商榷[J].中国药品标准,2019,20(6):486-489 |
《中国药典》2015年版中纯化水硝酸盐检查商榷 |
Discussion on nitrate detection of purified water in Chinese Pharmacopoeia 2015 edition |
投稿时间:2019-04-25 修订日期:2019-11-21 |
DOI: |
中文关键词: 硝酸盐 紫外-可见分光光度法 中国药典 纯化水 商榷 |
英文关键词: nitrate UV-Vis spectrophotometry Chinese Pharmacopoeia purified water discussion |
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中文摘要: |
目的:对《中国药典》2015年版二部纯化水中硝酸盐的检查方法提出意见建议。方法:按照标准考察了试剂“硫酸”对硝酸盐检查结果的影响,并首次建立了紫外-可见分光光度法作为硝酸盐检查的方法。结果:试剂“硫酸”的质量对硝酸盐比色法的检查影响很大,可采用紫外-可见分光光度法进一步测定。结论:紫外-可见分光光度法可作为《中国药典》纯化水中硝酸盐检查方法的重要补充。 |
英文摘要: |
Objective: To discuss the method of nitrate detection of purified water in Chinese Pharmacopoeia 2015。Methods:The effect of sulfuric acid are investigated on nitrate detection according to the standard ,and then establish the method of determination of nitrate by UV-Vis spectrophotometry.Results: There were obvious influence of purity of sulfuric acid by colorimetric method,and it can detect by UV-Vis spectrophotometry.Conclusion :It can be used as a supplementary method of UV-Vis spectrophotometry by Chinese Pharmacopoeia. |
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